dicalcium phosphate slurry rote production process

US5108728A

A process is disclosed for the production of granulated dicalcium phosphate dihydrate from fine-grained, powered dicalcium phosphate dihydrate, wherein 80 t0 95% of dicalcium phosphate dihydrate with a grain size of less than 120 μm and 20 to 5% of calcium hydroxide with a grain size of less than 120 μm are dry mixed and continuously …Web

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Process for the manufacture of dicalcium phosphate

The process for the production of a granular, animal feed grade, dicalcium phosphate product which comprises forming a slurry having a solids content between about 50% and about by weight of comminuted 2. The process of claim 1 wherein said phosphoric acid is preheated to a temperature between about 150 F. and the boiling point of said acid.Web

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Clean process for the production of defluorinated dicalcium phosphate

The process has essentially three main steps: phosphate rock digestion, defluorination and neutralization. In the first step a phosphate rock slurry is batch digested with concentrated sulfuric acid in the presence of some additives that retain the fluorine in the solution, as well as enable the adequate growth of the calcium sulfate crystals ...Web

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Clean process for the production of defluorinated dicalcium …

A new process for the production of defluorinated dicalcium phosphate using phosphate rock was developed. This new process has the main characteristic of being clean, without the production of any liquid waste.Web

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need process design of di calcium phosphate – Grinding Mill China

Dicalcium Phosphate – Wholesale Suppliers,Wholesale Products …. Catering to the process demands of varied applications, some of the industries …Di-calcium phosphate offered by us also finds its usage as a tableting agent in some … » Free Online Chat Dicalcium Phosphate-Dicalcium Phosphate Manufacturers, …. Dicalcium Phosphate …Web

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2023/sbm hcl with phosphate slurry.md at master

You've already forked 2023 0 Code Issues Pull Requests Packages Projects Releases Wiki ActivityWeb

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Recovery and separation of phosphorus as dicalcium phosphate …

In the wet phosphoric acid process, the phosphate rock is reacted with sulfuric acid (H 2 SO 4 ), producing gypsum (CaSO 4 ·2H 2 O) and aqueous phosphoric acid (reaction (1) …Web

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Process of making dicalcium phosphate.

2. In a method of making di-calcium phosphate, the steps. which consist intreating phosphate rock with hydrochloric acid under heat, cooling the mixture to about 30 C., treating the liquid product with calcium .hydroxid to secure amorphous di-calcium, phosphate, soluble in ammonium citrate and then separating the water insoluble neutral …Web

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Production of dicalcium phosphate or monocalcium phosphate

The invention claimed is: 1. A process for the production of dicalcium phosphate from a phosphate source material comprising the steps of: (a) preparing a solution of phosphoric acid by the action of a suitable mineral acid on a phosphate source material; (b) optionally separating the solution from residual solid materials; and (c) …Web

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OPINION AND REPORT on THE SAFETY OF DICALCIUM …

The typical dicalcium phosphate manufacturing process includes first a degreasing step of fine crushed bones in hot water (80° to 85°C). Regularly shaking removes a ... In the typical dicalcium production process, the liquor, after treatment with lime, will give a precipitate of dicalcium phosphate. ThisWeb

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Synthesis and Characterization of Feed-Grade Monocalcium Phosphate …

The monocalcium phosphate monohydrate is prepared from the PCC and phosphoric acid [ 5, 8 ]. A typical example can be illustrated as follows: 100 g of phosphoric acid, 85.44% H 3 PO 4, were diluted into 70.9 g of water to get a solution of 50% H 3 PO 4, and then the obtained solution was heated to 90°C in a water bath.Web

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Synthesis and Hydrolysis of Brushite (DCPD): The Role of Ionic

Brushite (dicalcium phosphate dihydrate, DCPD) is considered one of the possible precursors of the apatitic phase that constitutes the mineral component of bones, and it is often utilized in the preparation of biomaterials for hard tissue repair. In this work, we investigated the influence of ionic substitution on the synthesis, structure, and …Web

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What is Dicalcium Phosphate and How to Buy Dicalcium Phosphate …

In factories, Dicalcium Phosphate is made through the process of treating phosphate rock with nitric acid. The process for the production of Dicalcium Phosphate involves three main steps which include. Phosphate rock digestion; Deflourination process; Neutralization process; First. Phosphate rock is digested using concentrated sulfuric acid.Web

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Properties of sludge generated by the treatment of fluoride

Fluoride-containing wastewater is discharged from various industrial sites, including semiconductor, plating, and metal-treatment plants. To remove the fluoride, we treated wastewater with dicalcium phosphate dihydrate (DCPD, CaHPO 4 ·2H 2 O) to form fluorapatite [Ca 10 (PO 4) 6 F 2] crystals.We investigated the fluoride removal efficiency …Web

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(PDF) Synthesis of di-calcium phosphate used as feed additive for

The best values in terms of quality and quantity of dicalcium phosphate from locally phosphate rock were achieved at acid concentration of 10% w/w, reaction time of 1.5 hrs, at 30°C and pH values of 2.3-2.4 (during precipitation of impurities) and 5.5-5.6 (for the final synthesis of dicalcium phosphate).Web

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Dietary Phosphorus and Calcium Utilization in Growing Pigs

2.1.2. Mineral Phosphorus and Calcium. P is usually added to pig diets as dicalcium phosphate, which represents 60% of the feed phosphates used in the European Union; monocalcium and monodicalcium phosphates are also used ().Magnesium, calcium-magnesium, ammonium, and sodium phosphates are also available for use in livestock …Web

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Granular dicalcium phosphate product and method for the production …

The process which comprises reacting particulate, substantially fluorine-free dicalcium phosphate substantially free from iron and aluminum impurities with between about 2% and about 21% based on the weight of dicalcium phosphate of an acid selected from the group consisting of phosphoric acid, sulfuric acid, hydrochloric acid, and mixtures ...Web

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SYNTHESIS OF DICALCIUM PHOSPHATE USED AS …

synthesis of dicalcium phosphate). Pure dicalcium phosphate (98.20%) was prepared using above method. Purity of the dicalcium phosphate in terms of phosphorus content and total assay were ...Web

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Introducing the crystalline phase of dicalcium phosphate

Preparation and characterization of DCPM. Amorphous calcium hydrogen phosphate (ACHP), with a Ca/P atomic ratio of 1.0 38, which is identical to that of DCPM, was used as a precursor for the ...Web

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Dicalcium-Phosphates- Process, Technology, Applications, …

Process for preparing dicalcium phosphate containing fertilizer. Processing of dicalcium phosphate and sodium montmorillonite. Eggshell derived monocalcium and dicalcium …Web

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(PDF) Recovery and separation of phosphorus as dicalcium …

In this study, we develop an integrated process for the direct recovery and separation of dicalcium phosphate dihydrate for fertilizer and livestock feed additive …Web

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Production of dicalcium phosphate by treatment of phosphate …

Flow diagram of the process for production of dicalcium phosphate by the nitric acid route. 40 minutes at 50°C. The insoluble phase of acidulation was removed by …Web

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Phosphate Rock Properties

A typical process is described as follows: Calculated quantities of concentrated sulfuric acid (60° to 66° B.) diluted with weak phosphoric acid and a recirculated slurry of partly decomposed phosphate rock are fed continuously to one or more agitator tanks, then discharged into the first of a series of mixing tanks to which …Web

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Anhydrous calcium phosphate crystals stabilize DNA for dry …

The degradation of DNA is important for various areas of science and technology, including molecular biology, 1 medicine, 2 archeology 3,4 and more recently, digital data storage. 5,6 First investigations of the chemical decay of genetic material started soon after the revelation of the structure of DNA in the 1950s, paving the way for today's …Web

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Updated opinion and report on the safety of di- and tricalcium

The dicalcium phosphate production process as a whole will reduce the infectivity further up to 3.8 to 3.9 log10. This production should have resulted in a residual proteinaceous fraction not exceeding 0.60 % and with 98% of it having a …Web

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` June 2l, 1938; c. H. MILLIGAN I l 2,121,208 PRODUCTION …

the precipitated phosphate is "denned", that is, stored in bins, to complete the reaction. It has also been proposed to make an acid »solution of the acid phosphate, or a basic slurry of the acid phosphate, and remove the water by spray dry ing. Another proposal is to make a crystalline salt in the presence of excess dilute phosphoricWeb

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Production of defluorinated dicalcium phosphate from phosphate …

Abstract. A new process to produce defluorinated dicalcium phosphate (DCP) using phosphate rock concentrate has been developed. This new process has as main …Web

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Nitric acid acidulation of phosphate rock and pyrolysis of

Conventional production of wet-process phos- phoric acid involves the reaction of phosphate rock with sulfuric acid to produce a slurry con- sisting primarily of insoluble gypsum (CaSo 4 • 2H20 ) in dilute (26-30% P205) phosphoric ... may serve as a basis for the production of solid dicalcium phosphate and aqueous calcium nitrate by-product ...Web

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Engineering Conferences International ECI Digital Archives

New process to produce Di-calcium phosphate from low grade rock or tailing using diluted or by-product sulfuric acid. Gauthier Humblet. Prayon Technologies, Belgium, …Web

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Recovery and separation of phosphorus as dicalcium phosphate dihydrate

In this study, we develop an integrated process for the direct recovery and separation of dicalcium phosphate dihydrate for fertilizer and livestock feed additive production from a low-grade (2.0 wt% P) iron-rich (19.7 wt% Fe) phosphate ore. The process combines leaching using dilute sulfuric acid (0.29 M) and selective precipitation using ...Web

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Calcium feed phosphate production using the low-temperature …

Abstract. This article presents the restructuring effects of feed phosphate production in Poland. The new, wasteless and low-energy consuming dicalcium …Web

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Octacalcium phosphate (OCP)-based bone substitute materials

Calcium phosphate ceramics that have been reported to biodegrade in vivo are summarized in Table 1.Acidic calcium phosphates, such as dicalcium phosphate anhydrous (DCPA) and OCP, are classified as soluble ceramics at neutral pH 4, 14. α-TCP 4, 32 and amorphous calcium phosphate (ACP) 33, 34, 35 are recognized as highly …Web

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Patented Aug. 9, 1960.

The "wet process' acid, as produced, generally runs be tween about 26 and 30% P.O.5. Such dilute acid reacts poorly with limestone, and fails to give completeness of reaction such as to produce a product having substantially zero free acid in the dicalcium phosphate product. The "wet process' acid to be useful in the present process,Web

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Patented June 25, 1963

to heat a pH-adjusted dihydrate slurry. The mixing of boiling solutions of calcium salt and diammonium phosphate (DAP) or mono-ammonium phosphate (MAP), or adding a boiling DAP (or MAP) aqueous solution to a boiling calcium salt solution has been described in a U.S. patent disclosure, Serial No. 827,173, filed July 15, 1959, by Mooney et al. SuchWeb

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Method for producing feed grade dicalcium phosphate

The present invention discloses a method for producing feed grade mono-dicalcium phosphate. The present invention is characterized in that firstly, diluted phosphoric acid and a calcium containing compound carry out the liquid phase neutralizing reaction of step one in a reactor, and calcium biphosphate slurry is generated; then, a calcium containing …Web

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